diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

Base Information

Chemical Name:diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate
CAS No.:852949-01-0
Molecular Formula:C₂₄H₃₅O₅P
Molecular Weight:434.513
Hs Code.:

Synonyms:diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

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Chemical Property of diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

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Technology Process of diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

There total 4 articles about diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 852948-93-7
diethyl trans-2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]vinylphosphonate

: 852949-01-0
diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; for 5h;

Reference yield:

: 322472-55-9
3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)benzaldehyde

: 852949-01-0
diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 1 h / 20 °C

2.1: hydrogen / palladium on activated charcoal / ethanol; acetic acid / 5 h

With hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; ethanol; acetic acid;

Reference yield:

: 2233-18-3
4-hydroxy-3,5-dimethylbenzaldehyde

: 852949-01-0
diethyl 2-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]ethylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper; triethylamine / dichloromethane / 72 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

2.2: 1 h / 20 °C

3.1: hydrogen / palladium on activated charcoal / ethanol; acetic acid / 5 h

With hydrogen; copper; sodium hydride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; acetic acid;