(3R)-(-)-3-Phenylheptanal

Base Information

Chemical Name:(3R)-(-)-3-Phenylheptanal
CAS No.:75991-48-9
Molecular Formula:C₁₃H₁₈O
Molecular Weight:190.285
Hs Code.:

Synonyms:(3R)-(-)-3-Phenylheptanal

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Chemical Property of (3R)-(-)-3-Phenylheptanal

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Technology Process of (3R)-(-)-3-Phenylheptanal

There total 9 articles about (3R)-(-)-3-Phenylheptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18829-55-5
(E)-2-Heptenal

: 98-80-6
phenylboronic acid

: 72656-59-8
(3S)-3-phenylheptanal

: 75991-48-9
(3R)-(-)-3-Phenylheptanal

Guidance literature:: With potassium hydroxide; bis(ethylene)rhodium(I) chloride dimer; (1R,4R)-2,5-dibenzylbicyclo[2.2.1]hepta-2,5-diene; In tetrahydrofuran; methanol; water; at 10 ℃; for 6h; Title compound not separated from byproducts;
DOI:10.1246/cl.2005.1480

Reference yield:

: 84999-94-0
(R)-(-)-cinnamyl 2-methoxy-2-phenylpropyl ether

: 75991-48-9
(3R)-(-)-3-Phenylheptanal

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / t-BuOK/diisopropylamine/butyllithium / diethyl ether / -100 °C

2: aq. 40percent HClO₄ / diethyl ether

With n-butyllithium; perchloric acid; potassium tert-butylate; diisopropylamine; In diethyl ether;
DOI:10.1246/cl.1982.1637