ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate

Base Information

Chemical Name:ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate
CAS No.:950690-19-4
Molecular Formula:C₁₄H₂₁NO₄
Molecular Weight:267.325
Hs Code.:

Synonyms:ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate

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Chemical Property of ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate

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Technology Process of ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate

There total 66 articles about ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 891862-20-7
tert-butyl 4-bromo-7-oxo-6-azabicyclo[3.2.1]oct-2-ene-6-carboxylate

: 64-17-5
ethanol

: 950690-19-4
ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: With caesium carbonate; at 23 ℃; for 2h;
DOI:10.1021/ja0616433

Reference yield: 92.0%

: 1428733-31-6
ethyl (4R,5S)-5-(tert-butoxycarbonylamino)-4-(methylsulfonyloxy)cyclohex-1-enecarboxylate

: 950690-19-4
ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 20 ℃; for 0.0833333h;
DOI:10.1055/s-0032-1317948

Reference yield: 89.0%

: C₁₄H₂₃NO₆

: 950690-19-4
ethyl (S)-5-((tert-butoxycarbonyl)amino)cyclohexa-1,3-diene-1-carboxylate

Guidance literature:: C₁₄H₂₃NO₆; With pyridine; thionyl chloride; In dichloromethane; for 2h; Cooling with ice;

With magnesium iodide; In acetonitrile; for 0.166667h;