N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester

Base Information

Chemical Name:N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester
CAS No.:1172589-43-3
Molecular Formula:C₂₆H₃₀N₂O₆S
Molecular Weight:498.6
Hs Code.:

Synonyms:N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester

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Chemical Property of N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester

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Technology Process of N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester

There total 4 articles about N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95218-34-1
ethyl 2-{[(2,4-dimethoxyphenyl)methyl]amino}acetate

: 13950-62-4
ethyl 5-methyl-3-phenylisothiazole-4-carboxylate

: 1172589-43-3
N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester

Guidance literature:: ethyl 5-methyl-3-phenylisothiazole-4-carboxylate; With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 18h; Reflux;

ethyl 2-{[(2,4-dimethoxyphenyl)methyl]amino}acetate; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

Reference yield:

: 21486-57-7
2-(amino-phenyl-methylene)-3-oxo-butyric acid ethyl ester

: 1172589-43-3
N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: phosphorous (V) sulfide; chloranil / toluene / 20 °C / Reflux

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 18 h / Reflux

2.2: 20 h / 20 °C

With N-Bromosuccinimide; phosphorous (V) sulfide; chloranil; dibenzoyl peroxide; In tetrachloromethane; toluene;

Reference yield:

: 141-97-9
ethyl acetoacetate

: 1172589-43-3
N-(2,4-dimethoxy-benzyl),N-(ethyl ethanylat-2-yl)-5-aminomethyl-3-phenyl-isothiazole-4-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: tin(IV) chloride / benzene / 2.67 h / 20 °C / Reflux

2.1: phosphorous (V) sulfide; chloranil / toluene / 20 °C / Reflux

3.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 18 h / Reflux

3.2: 20 h / 20 °C

With N-Bromosuccinimide; phosphorous (V) sulfide; tin(IV) chloride; chloranil; dibenzoyl peroxide; In tetrachloromethane; toluene; benzene;