5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide

Base Information

Chemical Name:5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide
CAS No.:15762-04-6
Molecular Formula:C₁₀H₂₀O₆P₂S
Molecular Weight:330.279
Hs Code.:

Synonyms:5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide

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Chemical Property of 5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide

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Technology Process of 5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide

There total 3 articles about 5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 45734-11-0
2-hydroxy-2-thiono-5,5-dimethyl-1,3,2-dioxaphosphorinane

: 15762-04-6
5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide

: 1212-29-9
1,3-dicyclohexylthiourea

Guidance literature:: With dicyclohexyl-carbodiimide; In acetonitrile; Ambient temperature;
DOI:10.1021/jo00179a028

Reference yield: 98.0%

: 45734-11-0
2-hydroxy-2-thiono-5,5-dimethyl-1,3,2-dioxaphosphorinane

: 538-75-0
dicyclohexyl-carbodiimide

: 15762-04-6
5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide

: 1212-29-9
1,3-dicyclohexylthiourea

Guidance literature:: In acetonitrile; Mechanism; Product distribution; Ambient temperature;
DOI:10.1021/jo00179a028

Reference yield:

: 15995-44-5
Bis<5,5-dimethyl-2-oxo-P(V)-1,3,2-dioxaphosphorinan-2-yl> disulphide

: 15762-04-6
5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinan-2-yl 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl-oxide

: 4090-51-1
5,5,5',5'-tetramethyl-2,2'-oxy-bis-[1,3,2]dioxaphosphinane 2,2'-disulfide

Guidance literature:: With triphenylphosphine; In dichloromethane; Title compound not separated from byproducts; 1.) -70 deg C -> room temperature, 2.) room temperature, 30 min;