N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide
CAS No.:1569899-39-3
Molecular Formula:C₂₆H₄₉NO₄SSi₂
Molecular Weight:527.916
Hs Code.:

Synonyms:N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide

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Chemical Property of N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide

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Technology Process of N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 202974-92-3
N-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-4-methyl-benzenesulfonamide

: 485801-67-0
4-{[tert-butyl(dimethyl)silyl]oxy}-2-methylidenebutan-1-ol

: 1569899-39-3
N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/jo4027534

Reference yield: 95.0%

: 1569899-39-3
N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide

: 1569899-41-7
N-(4-hydroxy-2-methylenebutyl)-N-(2-hydroxyethyl)-4-methylbenzenesulfonamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo4027534

Reference yield:

: 1569899-39-3
N-(4-((tert-butyldimethylsilyl)oxy)-2-methylenebutyl)-N-(2-((tertbutyldimethylsilyl)oxy)ethyl)-4-methylbenzenesulfonamide

: 8-(o-tolyl)-4-tosyl-1,9-dioxa-4-azaspiro[5.5]undecane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / -50 °C / Inert atmosphere

With boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo4027534