(E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Base Information

Chemical Name:(E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone
CAS No.:179871-71-7
Molecular Formula:C₂₃H₂₈O₉
Molecular Weight:448.47
Hs Code.:

Synonyms:(E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

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Technology Process of (E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

There total 3 articles about (E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 36804-11-2
2,4,6-tri-MOM phloracetophenone

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 179871-71-7
(E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Guidance literature:: With potassium hydroxide; In methanol; for 15h; Ambient temperature;

Reference yield:

: 65490-09-7
2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone

: 179871-71-7
(E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH (80percent in oil) / 1.) THF, 0 deg C, 30 min; 2.) THF, 0 deg C, 30 min

2: 90 percent / KOH / methanol / 15 h / Ambient temperature

With potassium hydroxide; sodium hydride; In methanol;

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 179871-71-7
(E)-3-(3,4-Dimethoxy-phenyl)-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / N,N-diisopropylethylamine / tetrahydrofuran / 12 h / 0 °C

2: 1.) NaH (80percent in oil) / 1.) THF, 0 deg C, 30 min; 2.) THF, 0 deg C, 30 min

3: 90 percent / KOH / methanol / 15 h / Ambient temperature

With potassium hydroxide; sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol;