(5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]

Base Information

Chemical Name:(5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]
CAS No.:222736-63-2
Molecular Formula:C₂₄H₂₂O₆
Molecular Weight:406.435
Hs Code.:

Synonyms:(5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]

Suppliers and Price of (5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]

There total 2 articles about (5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 17893-46-8
2-(phenylselanyl)acetic acid

: 157363-85-4
1,2:5,6-Dianhydro-3,4-di-O-benzyl-D-mannitol

: 222736-63-2
(5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]

Guidance literature:: 2-(phenylselanyl)acetic acid; 1,2:5,6-Dianhydro-3,4-di-O-benzyl-D-mannitol; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 6.5h;

With acetic acid; In tetrahydrofuran; hexane; Heating;

With dihydrogen peroxide; acetic acid; In tetrahydrofuran; at 0 ℃; for 0.75h;
DOI:10.1021/jo026705w

Reference yield:

: phenylselenoacetic acid dianion

: 157363-85-4
1,2:5,6-Dianhydro-3,4-di-O-benzyl-D-mannitol

: 222736-63-2
(5R,5'R)-5,5'-[(1R,2R)-1,2-dibenzyloxyethane-1,2-diyl]bis[2(5H)-furanone]

Guidance literature:: With dihydrogen peroxide; acetic acid; Yield given; Multistep reaction; 2.) HOAc, heating; 3.) THF, 0 deg C, 2 h;
DOI:10.1016/S0040-4039(99)00172-0