7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

Base Information

Chemical Name:7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline
CAS No.:1225021-55-5
Molecular Formula:C₁₉H₁₆ClN₃O₃
Molecular Weight:369.807
Hs Code.:

Synonyms:7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

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Chemical Property of 7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

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Technology Process of 7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

There total 2 articles about 7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1225021-54-4
4,7-dichloro-2-(2-methylprop-1-enyl)-6-nitroquinazoline

: 5720-07-0
4-methoxyphenylboronic acid

: 1225021-55-5
7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

Guidance literature:: 4,7-dichloro-2-(2-methylprop-1-enyl)-6-nitroquinazoline; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 20 ℃; for 1h; Inert atmosphere;

4-methoxyphenylboronic acid; With sodium carbonate; In 1,2-dimethoxyethane; ethanol; at 80 ℃; for 3h; regioselective reaction; Microwave irradiation;
DOI:10.3390/molecules15052949

Reference yield: 45.0%

: 1225021-54-4
4,7-dichloro-2-(2-methylprop-1-enyl)-6-nitroquinazoline

: 5720-07-0
4-methoxyphenylboronic acid

: 1225021-55-5
7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

: 1225021-60-2
4,7-bis(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

Guidance literature:: 4,7-dichloro-2-(2-methylprop-1-enyl)-6-nitroquinazoline; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 20 ℃; for 1h; Inert atmosphere;

4-methoxyphenylboronic acid; With sodium carbonate; In 1,2-dimethoxyethane; ethanol; at 80 ℃; for 3h; regioselective reaction; Microwave irradiation;
DOI:10.3390/molecules15052949

Reference yield: 64.0%

: 1225021-55-5
7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline

: 98-80-6
phenylboronic acid

: 1225021-66-8
4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitro-7-phenylquinazoline

Guidance literature:: 7-chloro-4-(4-methoxyphenyl)-2-(2-methylprop-1-enyl)-6-nitroquinazoline; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

phenylboronic acid; With sodium carbonate; In ethanol; N,N-dimethyl-formamide; at 150 ℃; for 3h; Microwave irradiation;
DOI:10.3390/molecules15052949