benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside
CAS No.:114669-83-9
Molecular Formula:C₃₆H₄₅NO₁₁
Molecular Weight:667.753
Hs Code.:

Synonyms:benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

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Chemical Property of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

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Technology Process of benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

There total 10 articles about benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

: benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(3,4-O-isopropylidene-2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

: 114669-83-9
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

Guidance literature:: With acetic acid; at 98 ℃; for 1h;
DOI:10.1016/0008-6215(87)80274-4

Reference yield: 85.0%

: 114669-70-4
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-<3,4,6-tri-O-acetyl-2-O-methyl-β-D-galactopyranosyl>-α-D-glucopyranoside

: 114669-83-9
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; for 1h; Ambient temperature;
DOI:10.1016/0008-6215(87)80274-4

Reference yield:

: 10357-31-0
3,4,6-tri-O-acetyl-2-O-methyl-α-D-galactopyranosyl bromide

: 114669-83-9
benzyl 2-acetamido-3,6-di-O-benzyl-2-deoxy-4-O-(2-O-methyl-β-D-galactopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 39.7 percent / mercuric cyanide / acetonitrile / 5 h / Ambient temperature

2: 85 percent / sodium methoxide / methanol / 1 h / Ambient temperature

With sodium methylate; mercury(II) cyanide; In methanol; acetonitrile;
DOI:10.1016/0008-6215(87)80274-4