C₁₂⁽¹³⁾CH₁₇NO

Base Information

Chemical Name:C₁₂⁽¹³⁾CH₁₇NO
CAS No.:142439-17-6
Molecular Formula:C₁₃H₁₇NO
Molecular Weight:204.273
Hs Code.:

C<sub>12</sub><sup>(13)</sup>CH<sub>17</sub>NO

Synonyms:C₁₂⁽¹³⁾CH₁₇NO

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Chemical Property of C₁₂⁽¹³⁾CH₁₇NO

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Technology Process of C₁₂⁽¹³⁾CH₁₇NO

There total 4 articles about C₁₂⁽¹³⁾CH₁₇NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 142439-16-5
2-(1-piperidinyl)acetophenone-13C

: 142439-17-6
C₁₂⁽¹³⁾CH₁₇NO

Guidance literature:: With dicobalt octacarbonyl; dodecacarbonyl-triangulo-triruthenium; carbon monoxide; In benzene; at 200 - 220 ℃; for 72h; under 41040 Torr;
DOI:10.1021/ja00044a010

Reference yield:

: 110-89-4
piperidine

: 142439-17-6
C₁₂⁽¹³⁾CH₁₇NO

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h, 2.) ether, hexane, RT, overnight

2: 90 percent / CO, Co₂(CO)8, Ru₃(CO)12 / benzene / 72 h / 200 - 220 °C / 41040 Torr

With n-butyllithium; dicobalt octacarbonyl; dodecacarbonyl-triangulo-triruthenium; carbon monoxide; In benzene;
DOI:10.1021/ja00044a010

Reference yield:

: 10383-88-7
acetophenone-13C=O

: 142439-17-6
C₁₂⁽¹³⁾CH₁₇NO

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / (C₄H₉)4NBr₃ / CH₂Cl₂; methanol / Ambient temperature

2: 1.) n-BuLi / 1.) ether, hexane, RT, 1 h, 2.) ether, hexane, RT, overnight

3: 90 percent / CO, Co₂(CO)8, Ru₃(CO)12 / benzene / 72 h / 200 - 220 °C / 41040 Torr

With n-butyllithium; dicobalt octacarbonyl; dodecacarbonyl-triangulo-triruthenium; carbon monoxide; tetra-N-butylammonium tribromide; In methanol; dichloromethane; benzene;
DOI:10.1021/ja00044a010