chloromethyl(dicyclohexyl)phosphine oxide

Base Information

Chemical Name:chloromethyl(dicyclohexyl)phosphine oxide
CAS No.:16523-55-0
Molecular Formula:C₁₃H₂₄ClOP
Molecular Weight:262.76
Hs Code.:

Synonyms:chloromethyl(dicyclohexyl)phosphine oxide

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Chemical Property of chloromethyl(dicyclohexyl)phosphine oxide

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Technology Process of chloromethyl(dicyclohexyl)phosphine oxide

There total 2 articles about chloromethyl(dicyclohexyl)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 34729-69-6
dicyclohexyl(hydroxymethyl)phosphine oxide

: 16523-55-0
chloromethyl(dicyclohexyl)phosphine oxide

Guidance literature:: With phosphorus pentachloride; In chloroform; toluene; at 60 ℃; for 24h; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0036-1591546

Reference yield:

: 14717-29-4
dicyclohexylphosphine oxide

: 16523-55-0
chloromethyl(dicyclohexyl)phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 24 h / 60 °C / Inert atmosphere; Schlenk technique

2: phosphorus pentachloride / chloroform; toluene / 24 h / 60 °C / Inert atmosphere; Schlenk technique

With phosphorus pentachloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; chloroform; toluene;
DOI:10.1055/s-0036-1591546