diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate

Base Information

Chemical Name:diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate
CAS No.:930766-90-8
Molecular Formula:C₁₉H₃₁O₆P
Molecular Weight:386.425
Hs Code.:

Synonyms:diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate

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Chemical Property of diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate

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Technology Process of diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate

There total 5 articles about diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 930766-89-5
4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl alcohol

: 930766-90-8
diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CH₂Cl₂ / 21.5 h / 0 - 20 °C

2: sodium iodide / acetone / 22 h

3: 168 mg / 6.5 h / 100 °C

With triethylamine; sodium iodide; In dichloromethane; acetone; 3: Arbuzov reaction;
DOI:10.1016/j.bmcl.2006.11.096

Reference yield:

: methanesulfonic acid 3-methoxy-5-methoxymethoxy-4-(3-methyl-but-2-enyl)-benzyl ester

: 930766-90-8
diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium iodide / acetone / 22 h

2: 168 mg / 6.5 h / 100 °C

With sodium iodide; In acetone; 2: Arbuzov reaction;
DOI:10.1016/j.bmcl.2006.11.096

Reference yield:

: 126809-66-3
(3-Methoxy-5-methoxymethoxy-phenyl)-methanol

: 930766-90-8
diethyl (4-(3-methyl-2-butenyl)-3-methoxy-5-(methoxymethoxy)benzyl)phosphonate

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-BuLi; TMEDA / tetrahydrofuran; hexane / 1 h / -20 °C

1.2: CuBr*DMS / tetrahydrofuran / 1 h / -20 °C

1.3: 43 percent / tetrahydrofuran / 2 h / -20 °C

2.1: triethylamine / CH₂Cl₂ / 21.5 h / 0 - 20 °C

3.1: sodium iodide / acetone / 22 h

4.1: 168 mg / 6.5 h / 100 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; triethylamine; sodium iodide; In tetrahydrofuran; hexane; dichloromethane; acetone; 4.1: Arbuzov reaction;
DOI:10.1016/j.bmcl.2006.11.096