2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole

Base Information

Chemical Name:2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole
CAS No.:1309377-85-2
Molecular Formula:C₁₂H₁₄BrNO
Molecular Weight:268.153
Hs Code.:

Synonyms:2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole

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Chemical Property of 2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole

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Technology Process of 2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole

There total 5 articles about 2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: C₁₂H₁₆BrNO₂

: 1309377-85-2
2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole

Guidance literature:: With thionyl chloride; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/pola.24692

Reference yield: 78.0%

: 79568-30-2
4,4-dimethyl-2-p-tolyl-2-oxazoline

: 1309377-85-2
2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; at 100 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1039/c8ob01072b

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 1309377-85-2
2-[4-(bromomethyl)phenyl]-4,5-dihydro-4,4-dimethyloxazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 18 h / 25 °C / Molecular sieve; Inert atmosphere; Schlenk technique

1.2: 4 h / 25 °C / Molecular sieve; Inert atmosphere; Schlenk technique

2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 5 h / 100 °C / Inert atmosphere; Schlenk technique

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; dichloromethane;
DOI:10.1039/c8ob01072b