Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate

Base Information

Chemical Name:Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate
CAS No.:475272-86-7
Molecular Formula:C₄₀H₃₂N₆O₉
Molecular Weight:740.729
Hs Code.:

Synonyms:Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate

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Chemical Property of Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate

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Technology Process of Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate

There total 11 articles about Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 475272-86-7
Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate

Guidance literature:

Reference yield:

: 16013-85-7,136901-10-5
2,6-dicholoro-3-nitropyridine

: 475272-86-7
Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 9 steps

1.1: NH₃ / ethanol

1.2: NaNO₂; H₂SO₄

1.3: H₂O

2.1: Ag₂CO₃

3.1: [Pd(PPh₃)4]

4.1: O₃ / acetic acid

4.2: AgNO₃; KOH

5.1: PTSA

6.1: H₂ / PtO₂

7.1: DIEA

8.1: H₂ / PtO₂

9.1: DIEA

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonia; hydrogen; toluene-4-sulfonic acid; ozone; N-ethyl-N,N-diisopropylamine; silver carbonate; platinum(IV) oxide; In ethanol; acetic acid;
DOI:10.1002/anie.200390154

Reference yield:

: 475272-63-0
5-nitro-6-phenylmethoxypyridine-2-carboxylic acid

: 475272-86-7
Methyl 6-(benzyloxy)-5-{[(6-(benzyloxy)-5-{[(6-(benzyloxy)-5-nitro-2-pyridinyl)carbonyl]amino}-2-pyridinyl)carbonyl]amino}-2-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: PTSA

2: H₂ / PtO₂

3: DIEA

4: H₂ / PtO₂

5: DIEA

With hydrogen; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide;
DOI:10.1002/anie.200390154