dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate

Base Information

• Chemical Name: dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate
• CAS No.: 89691-00-9
• Molecular Formula: BF₄*C₄₄H₃₈Cl₂IrP₂
• Molecular Weight: 978.664

Synonyms:dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate

Chemical Property of dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate

Chemical Property:

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Technology Process of dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate

There total 1 articles about dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

[Ir(hydrido)2(acetone)2(triphenylphosphine)2](BF4) (82582-67-0,72414-17-6) + 2,6-dichlorostyrene (28469-92-3) → dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate (89691-00-9)

Guidance literature:

In dichloromethane; to soln. of Ir complex in CH2Cl2 added excess of arene, stirred at 15°C for 15 min; evapd. in vac., washed with ether/pentane, dried in vac., recrystd. from CH2Cl2/Et2O;

DOI:10.1021/ja00322a029

Reference yield:

dihydrido(η3(Cl,C,C)-2,6-dichlorostyrene)bis(triphenylphosphine)iridium(III) tetrafluoroborate (89691-00-9) → [Ir(Cl2C6H3C2H5)(P(C6H5)3)2](1+)*BF4(1-)=[Ir(Cl2C6H3C2H5)(P(C6H5)3)2]BF4 (89690-92-6)

Guidance literature:

In not given; heating to 40°C for 15 min;

DOI:10.1021/ja00322a029

upstream raw materials:

[Ir(hydrido)2(acetone)2(triphenylphosphine)2](BF4)

2,6-dichlorostyrene

Downstream raw materials:

[Ir(Cl₂C₆H₃C₂H₅)(P(C₆H₅)3)2]⁽¹⁺⁾*BF₄^(1-)=[Ir(Cl₂C₆H₃C₂H₅)(P(C₆H₅)3)2]BF₄

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