succinimido-p-benzyl-dihydrocinnamate

Base Information

Chemical Name:succinimido-p-benzyl-dihydrocinnamate
CAS No.:277332-37-3
Molecular Formula:C₂₀H₁₉NO₄
Molecular Weight:337.375
Hs Code.:

Synonyms:succinimido-p-benzyl-dihydrocinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of succinimido-p-benzyl-dihydrocinnamate

Chemical Property:

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Technology Process of succinimido-p-benzyl-dihydrocinnamate

There total 2 articles about succinimido-p-benzyl-dihydrocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 147740-88-3
succinimido-p-benzoylcinnamate

: 277332-37-3
succinimido-p-benzyl-dihydrocinnamate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 24h; under 2585.74 Torr;
DOI:10.1016/S0960-894X(00)00043-3

Reference yield:

: 74839-99-9
p-benzoylcinnamic acid

: 277332-37-3
succinimido-p-benzyl-dihydrocinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Et₃N / acetonitrile / 16 h / 20 °C

2: 69 percent / H₂ / 10 percent Pd/C / ethyl acetate / 24 h / 2585.74 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; acetonitrile; 1: Condensation / 2: Hydrogenation;
DOI:10.1016/S0960-894X(00)00043-3

Reference yield:

: 277332-37-3
succinimido-p-benzyl-dihydrocinnamate

: Phosphoric acid 4-amino-butyl ester (2R,3S,4S,5R)-3,4,5,6-tetrahydroxy-tetrahydro-pyran-2-ylmethyl ester

: BnDC-Glc-6-P

: BnDC-Glc-6-P

Guidance literature:: With TEAB buffer; In N,N-dimethyl-formamide; at 20 ℃; for 24h; pH=8.0; Title compound not separated from byproducts;
DOI:10.1016/S0960-894X(00)00043-3