succinimido-p-benzoylcinnamate

Base Information

• Chemical Name: succinimido-p-benzoylcinnamate
• CAS No.: 147740-88-3
• Molecular Formula: C₂₀H₁₅NO₅
• Molecular Weight: 349.343
• Mol file: 147740-88-3.mol

Synonyms:succinimido-p-benzoylcinnamate

Chemical Property of succinimido-p-benzoylcinnamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of succinimido-p-benzoylcinnamate

There total 1 articles about succinimido-p-benzoylcinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

p-benzoylcinnamic acid (74839-99-9) + diphenyl succinimidyl phosphate → succinimido-p-benzoylcinnamate (147740-88-3)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 16h;

DOI:10.1016/S0960-894X(00)00043-3

Reference yield: 69.0%

succinimido-p-benzoylcinnamate (147740-88-3) → succinimido-p-benzyl-dihydrocinnamate (277332-37-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 24h; under 2585.74 Torr;

DOI:10.1016/S0960-894X(00)00043-3

Reference yield:

succinimido-p-benzoylcinnamate (147740-88-3) → BnDC-Glc-6-P

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / H₂ / 10 percent Pd/C / ethyl acetate / 24 h / 2585.74 Torr

2: TEAB buffer / dimethylformamide / 24 h / 20 °C / pH 8.0

With TEAB buffer; hydrogen; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; 1: Hydrogenation / 2: Condensation;

DOI:10.1016/S0960-894X(00)00043-3

upstream raw materials:

p-benzoylcinnamic acid

Downstream raw materials:

succinimido-p-benzyl-dihydrocinnamate

Refernces