O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

Base Information

Chemical Name:O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine
CAS No.:917376-74-0
Molecular Formula:C₃₉H₃₂N₆O₁₀
Molecular Weight:744.717
Hs Code.:

O<sup>6</sup>-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

Synonyms:O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

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Chemical Property of O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

Chemical Property:

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Technology Process of O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

There total 6 articles about O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {6-[2-(4-nitro-phenyl)-ethoxy]-9-trimethylsilanyl-9H-purin-2-yl}-trimethylsilanyl-amine

: 57236-69-8
(3S,4R,5R)-2-acetoxy-5-((benzoyloxy)methyl)tetrahydrofuran-3,4-diyl dibenzoate

: 917376-74-0
O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

Guidance literature:: With trimethylsilyl trifluorosulfonate; In toluene; at 80 ℃; for 8h;
DOI:10.1080/15257770500267113

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 917376-74-0
O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / triphenylphosphine; ethyl azodicarboxylate / dioxane / 24 h

2: 69 percent / HCl / methanol / 48 h / 20 °C

3: CH₂Cl₂ / 2 h / 80 °C

4: 14.6 g / trimethylsilyl trifluorosulfonate / toluene / 8 h / 80 °C

With hydrogenchloride; ethyl azodicarboxylate; trimethylsilyl trifluorosulfonate; triphenylphosphine; In 1,4-dioxane; methanol; dichloromethane; toluene;
DOI:10.1080/15257770500267113

Reference yield:

: 3056-33-5
2,9-diacetylguanine

: 917376-74-0
O⁶-[2-(4-nitrophenyl)ethyl]-9-(2,3,5-tri-O-benzoyl-α-D-arabinofuranosyl)guanine

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / triphenylphosphine; ethyl azodicarboxylate / dioxane / 24 h

2: 69 percent / HCl / methanol / 48 h / 20 °C

3: CH₂Cl₂ / 2 h / 80 °C

4: 14.6 g / trimethylsilyl trifluorosulfonate / toluene / 8 h / 80 °C

With hydrogenchloride; ethyl azodicarboxylate; trimethylsilyl trifluorosulfonate; triphenylphosphine; In 1,4-dioxane; methanol; dichloromethane; toluene;
DOI:10.1080/15257770500267113