N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride

Base Information

Chemical Name:N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride
CAS No.:1335405-10-1
Molecular Formula:C₂₀H₂₅BrN₂O₄S*ClH
Molecular Weight:505.86
Hs Code.:

Synonyms:N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride

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Chemical Property of N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride

Chemical Property:

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Technology Process of N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride

There total 9 articles about N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1335407-03-8
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

: 1335405-10-1
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 25 ℃; for 1h;

Reference yield:

: 14815-12-4
N-(2-methoxyphenyl)-2,2,2-trifluoro-acetamide

: 1335405-10-1
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: chlorosulfonic acid / dichloromethane / 0 - 30 °C

2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 20 h / Inert atmosphere; Reflux

3.1: sodium hydroxide; water / methanol / 5 - 70 °C

4.1: sodium sulfate; acetic acid / 4 h / 27 °C / Inert atmosphere

4.2: 1 h / 20 - 30 °C

4.3: 10 °C / pH 9

5.1: hydrogenchloride / methanol / 1 h / 25 °C

With hydrogenchloride; chlorosulfonic acid; aluminum (III) chloride; water; acetic acid; sodium sulfate; sodium hydroxide; In methanol; dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 1184086-20-1
4-methoxy-3-(2,2,2-trifluoroacetamido)benzenesulfonyl chloride

: 1335405-10-1
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 20 h / Inert atmosphere; Reflux

2.1: sodium hydroxide; water / methanol / 5 - 70 °C

3.1: sodium sulfate; acetic acid / 4 h / 27 °C / Inert atmosphere

3.2: 1 h / 20 - 30 °C

3.3: 10 °C / pH 9

4.1: hydrogenchloride / methanol / 1 h / 25 °C

With hydrogenchloride; aluminum (III) chloride; water; acetic acid; sodium sulfate; sodium hydroxide; In methanol; 1,2-dichloro-ethane;