N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

Base Information

Chemical Name:N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine
CAS No.:1335407-03-8
Molecular Formula:C₂₀H₂₅BrN₂O₄S
Molecular Weight:469.399
Hs Code.:

Synonyms:N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

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Chemical Property of N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

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Technology Process of N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

There total 8 articles about N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1445-73-4
1-Methyl-4-piperidone

: 1335407-01-6
5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyaniline

: 1335407-03-8
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

Guidance literature:: 1-Methyl-4-piperidone; 5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyaniline; With acetic acid; sodium sulfate; at 27 ℃; for 4h; Inert atmosphere;

With sodium tris(acetoxy)borohydride; at 20 - 30 ℃; for 1h;

With sodium hydroxide; In water; at 10 ℃; pH=9;

Reference yield:

: C₂₀H₂₃BrN₂O₄S

: 1335407-03-8
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

Guidance literature:: With sodium tris(acetoxy)borohydride; at 20 - 25 ℃; for 2.08333h;

Reference yield:

: 14815-12-4
N-(2-methoxyphenyl)-2,2,2-trifluoro-acetamide

: 1335407-03-8
N-[5-(5-bromo-2-methoxybenzenesulfonyl)-2-methoxyphenyl]-N-(1-methylpiperidin-4-yl)amine

Guidance literature:: Multi-step reaction with 4 steps

1.1: chlorosulfonic acid / dichloromethane / 0 - 30 °C

2.1: aluminum (III) chloride / 1,2-dichloro-ethane / 20 h / Inert atmosphere; Reflux

3.1: sodium hydroxide; water / methanol / 5 - 70 °C

4.1: sodium sulfate; acetic acid / 4 h / 27 °C / Inert atmosphere

4.2: 1 h / 20 - 30 °C

4.3: 10 °C / pH 9

With chlorosulfonic acid; aluminum (III) chloride; water; acetic acid; sodium sulfate; sodium hydroxide; In methanol; dichloromethane; 1,2-dichloro-ethane;