Technology Process of 4,5-diiodophthaldiamide
There total 5 articles about 4,5-diiodophthaldiamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium hydroxide;
at 50 - 60 ℃;
for 1.5h;
DOI:10.1021/jo9521662
- Guidance literature:
-
Multi-step reaction with 2 steps
1: fuming sulphuric acid; iodine / 24 h / 70 °C
2: ammonium hydroxide / 1.5 h / 60 °C
With
ammonium hydroxide; fuming sulphuric acid; iodine;
DOI:10.1039/c4ob00901k
- Guidance literature:
-
Multi-step reaction with 4 steps
1: periodic acid; iodine / acetic acid; sulfuric acid; water / 24 h / 60 - 65 °C
2: potassium permanganate / pyridine; 2,2,2-trifluoroethanol / 192 h / 40 °C
3: formamide / 0.58 h / 180 °C
4: ammonium hydroxide / water / 1.5 h / 60 °C
With
ammonium hydroxide; potassium permanganate; iodine; formamide; periodic acid;
In
pyridine; 2,2,2-trifluoroethanol; sulfuric acid; water; acetic acid;
DOI:10.1002/chem.201803316
