4,5-diiodophthaldiamide

Base Information

Chemical Name:4,5-diiodophthaldiamide
CAS No.:175883-97-3
Molecular Formula:C₈H₆I₂N₂O₂
Molecular Weight:415.957
Hs Code.:

Synonyms:4,5-diiodophthaldiamide

Suppliers and Price of 4,5-diiodophthaldiamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4,5-diiodophthaldiamide

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 4,5-diiodophthaldiamide

There total 5 articles about 4,5-diiodophthaldiamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 68218-30-4
4,5-diiodophthalimide

: 175883-97-3
4,5-diiodophthaldiamide

Guidance literature:: With ammonium hydroxide; at 50 - 60 ℃; for 1.5h;
DOI:10.1021/jo9521662

Reference yield:

: 136918-14-4,85-41-6
phthalimide

: 175883-97-3
4,5-diiodophthaldiamide

Guidance literature:: Multi-step reaction with 2 steps

1: fuming sulphuric acid; iodine / 24 h / 70 °C

2: ammonium hydroxide / 1.5 h / 60 °C

With ammonium hydroxide; fuming sulphuric acid; iodine;
DOI:10.1039/c4ob00901k

Reference yield:

: 95-47-6
o-xylene

: 175883-97-3
4,5-diiodophthaldiamide

Guidance literature:: Multi-step reaction with 4 steps

1: periodic acid; iodine / acetic acid; sulfuric acid; water / 24 h / 60 - 65 °C

2: potassium permanganate / pyridine; 2,2,2-trifluoroethanol / 192 h / 40 °C

3: formamide / 0.58 h / 180 °C

4: ammonium hydroxide / water / 1.5 h / 60 °C

With ammonium hydroxide; potassium permanganate; iodine; formamide; periodic acid; In pyridine; 2,2,2-trifluoroethanol; sulfuric acid; water; acetic acid;
DOI:10.1002/chem.201803316