C₄₄H₇₆O₁₀Si₃

Base Information

Chemical Name:C₄₄H₇₆O₁₀Si₃
CAS No.:153145-45-0
Molecular Formula:C₄₄H₇₆O₁₀Si₃
Molecular Weight:849.338
Hs Code.:

C<sub>44</sub>H<sub>76</sub>O<sub>10</sub>Si<sub>3</sub>

Synonyms:C₄₄H₇₆O₁₀Si₃

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Chemical Property of C₄₄H₇₆O₁₀Si₃

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Technology Process of C₄₄H₇₆O₁₀Si₃

There total 13 articles about C₄₄H₇₆O₁₀Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-45-0
C₄₄H₇₆O₁₀Si₃

Guidance literature:: Multi-step reaction with 6 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 80 percent / OsO₄, pyridine / diethyl ether / 12 h / 0 °C

6: Et₃N / -78 °C

With pyridine; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In diethyl ether; dichloromethane;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-45-0
C₄₄H₇₆O₁₀Si₃

Guidance literature:: Multi-step reaction with 13 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 80 percent / OsO₄, pyridine / diethyl ether / 12 h / 0 °C

13: Et₃N / -78 °C

With pyridine; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; ozone; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 153145-56-3
C₃₃H₅₆O₈Si₂

: 153145-45-0
C₄₄H₇₆O₁₀Si₃

Guidance literature:: Multi-step reaction with 12 steps

1: KMnO₄, KH₂PO₄

3: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

4: 100 percent / p-TsOH

5: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

6: acid

7: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

8: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

9: 95 percent / CH₂Cl₂ / 15 h / -45 °C

10: 63 percent / Burgess' reagent

11: 80 percent / OsO₄, pyridine / diethyl ether / 12 h / 0 °C

12: Et₃N / -78 °C

With pyridine; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;