4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone

Base Information

Chemical Name:4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone
CAS No.:503132-37-4
Molecular Formula:C₁₅H₁₄F₂N₂O₃S
Molecular Weight:340.351
Hs Code.:

Synonyms:4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone

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Chemical Property of 4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone

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Technology Process of 4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone

There total 1 articles about 4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 73960-07-3
4-difluoromethoxybenzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 503132-37-4
4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone

Guidance literature:: In methanol; for 2h;

Reference yield: 98.0%

: 503132-37-4
4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone

: 4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone sodium salt

Guidance literature:: With sodium methylate; In methanol; for 1h;

Reference yield:

: 503132-37-4
4-difluoromethoxy-phenyl benzaldehyde-tosylhydrazone

: cis-N-[2-(difluoromethoxy-phenyl)-cyclopropyl]-2-trifluoromethyl-benzamide

: N-[trans-2-(4-difluoromethoxyphenyl)cyclopropyl]-2-trifluoromethylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 1 h

2: dirhodium tetraacetate; N-benzyl-N,N,N-triethylammonium chloride / 1,4-dioxane / 2 h / 20 - 60 °C

With dirhodium tetraacetate; N-benzyl-N,N,N-triethylammonium chloride; sodium methylate; In 1,4-dioxane; methanol;