(4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

Base Information

Chemical Name:(4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane
CAS No.:883884-89-7
Molecular Formula:C₃₅H₃₇BO₄
Molecular Weight:532.487
Hs Code.:

Synonyms:(4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

Suppliers and Price of (4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of (4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

There total 8 articles about (4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1044871-05-7
(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

: 883884-89-7
(4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

Guidance literature:: With copper(I) thiophene-2-carboxylate; O,O'-(1,1'-biphenyl-2,2'-diyl)-N,N'-bis[(S,S)-1-phenyl-ethyl]phosphoramidite; In dichloromethane; at -80 ℃; for 4h; Schlenk technique;
DOI:10.1002/anie.201509198

Reference yield: 68.0%

: 883884-87-5
(3S,4'R,5'R)-3-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]pent-4-en-1-yl methanesulfonate

: 883884-89-7
(4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

Guidance literature:: (3S,4'R,5'R)-3-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]pent-4-en-1-yl methanesulfonate; With lithium triethylborohydride; In tetrahydrofuran; at 20 ℃; for 1h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1055/s-2005-921756

Reference yield:

: 1044871-05-7
(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

: 883884-89-7
(4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(pent-1-en-3-yl)-1,3,2-dioxaborolane

: 883884-90-0
(3R,4'R,5'R)-3-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]pent-1-ene

: C₃₅H₃₇BO₄

Guidance literature:: With copper(I) thiophene-2-carboxylate; N,N-bis-[(S)-1-phenylethyl]dibenzo[d,f][1,3,2]dioxaphosphepin-6-amine; In dichloromethane; at 6 ℃; for 78h; Reagent/catalyst;
DOI:10.1002/anie.201509198