(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

Base Information

Chemical Name:(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene
CAS No.:1044871-05-7
Molecular Formula:C₃₃H₃₂BClO₄
Molecular Weight:538.879
Hs Code.:

Synonyms:(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

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Chemical Property of (4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

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Technology Process of (4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

There total 2 articles about (4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 130874-89-4
(2R,3R)-1,4-dimethoxy-1,1,4,4-tetraphenyl-2,3-butandiol

: 491879-29-9
trans-2-(chloromethyl)ethenylboronic acid

: 1044871-05-7
(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

Guidance literature:: In toluene; at 80 ℃; Molecular sieve;
DOI:10.1002/anie.201509198

Reference yield: 57.0%

: 1044870-99-6
(4''R,5''R,2'E)-3'-[4'',5''-bis(methoxydiphenylmethyl)-1'',3'',2''-dioxaborolan-2''-yl]-2'-propen-1'-yl 2,2,2-trichloroacetimidate

: 1044871-05-7
(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In tetrahydrofuran; at 80 ℃; for 23h;
DOI:10.1002/chem.200800034

Reference yield: 92.0%

: 1044871-05-7
(4'R,5'R,1E)-1-[4',5'-bis(methoxydiphenylmethyl)-1',3',2'-dioxaborolan-2'-yl]-3-chloro-2-propene

: 693-25-4
n-pentylmagnesium bromide

: (4R,5R,3’S)-4,5-bis(methoxydiphenylmethyl)-2-(oct-1-en-3-yl)-1,3,2-dioxaborolane

Guidance literature:: With copper(I) thiophene-2-carboxylate; O,O'-(1,1'-biphenyl-2,2'-diyl)-N,N'-bis[(S,S)-1-phenyl-ethyl]phosphoramidite; In dichloromethane; at -80 ℃; for 4h; Schlenk technique;
DOI:10.1002/anie.201509198