N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide

Base Information

Chemical Name:N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide
CAS No.:147865-11-0
Molecular Formula:C₂₁H₁₈ClN₃O₂S
Molecular Weight:411.912
Hs Code.:

N<sub>1</sub>-[2-(biphenyl-4-yloxy)ethanoyl]-N<sub>4</sub>-(4-chlorophenyl)-thiosemicarbazide

Synonyms:N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide

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Chemical Property of N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide

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Technology Process of N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide

There total 3 articles about N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 84161-08-0
2-(biphenyl-4-yloxy)acetic acid hydrazide

: 147865-11-0
N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide

Guidance literature:: In ethanol; for 4h; Heating;
DOI:10.1002/jps.2600820210

Reference yield:

: 92-69-3
4-Phenylphenol

: 147865-11-0
N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / acetone / 20 h / Heating

2: 99percent hydrazine hydrate / ethanol / 10 h / Heating

3: 95 percent / aq. ethanol / 4 h / Heating

With potassium carbonate; hydrazine hydrate; In ethanol; acetone;
DOI:10.1002/jps.2600820210

Reference yield:

: 54334-74-6
ethyl 2-(biphenyl-4-yloxy)acetate

: 147865-11-0
N₁-[2-(biphenyl-4-yloxy)ethanoyl]-N₄-(4-chlorophenyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 99percent hydrazine hydrate / ethanol / 10 h / Heating

2: 95 percent / aq. ethanol / 4 h / Heating

With hydrazine hydrate; In ethanol;
DOI:10.1002/jps.2600820210