N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine

Base Information

• Chemical Name: N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine
• CAS No.: 1263089-90-2
• Molecular Formula: C₂₄H₁₇F₃N₂O
• Molecular Weight: 406.407

Synonyms:N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine

Chemical Property of N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine

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Technology Process of N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine

There total 2 articles about N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-Trifluoromethylbenzaldehyde (455-19-6) + phenyl(5-phenyl-isoxazol-3-yl)methanamine (1263089-84-4) → N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine (1263089-90-2)

Guidance literature:

With acetic acid; at 20 ℃; for 12h;

DOI:10.1039/c0ob00511h

Reference yield:

4-Trifluoromethylbenzaldehyde (455-19-6) + phenyl(5-phenyl-1,2-oxazol-3-yl)methanone (3672-49-9) → N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine (1263089-90-2)

Guidance literature:

phenyl(5-phenyl-1,2-oxazol-3-yl)methanone; With benzylamine; In toluene; at 60 ℃;

4-Trifluoromethylbenzaldehyde; In acetic acid;

DOI:10.1021/ol3013414

Reference yield: 95.0%

N-(4-trifluoromethylbenzylidene)-phenyl-(5-phenyl-isoxazol-3-yl)methanamine (1263089-90-2) → 2-(4-trifluoromethylphenyl)-4(5)-phenacyl-5(4)-phenyl-imidazole (1263090-00-1)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; at 20 ℃; for 8h; Inert atmosphere;

DOI:10.1039/c0ob00511h

upstream raw materials:

4-Trifluoromethylbenzaldehyde

phenyl(5-phenyl-isoxazol-3-yl)methanamine

phenyl(5-phenyl-1,2-oxazol-3-yl)methanone

Downstream raw materials:

2-(4-trifluoromethylphenyl)-4⁽⁵⁾-phenacyl-5⁽⁴⁾-phenyl-imidazole

2-(4-trifluoromethylphenyl)-5,2',5'-triphenyl-4,4'-biimidazole

1-[2-(4-trifluoromethylphenyl)-5-phenyl-1H-imidazol-4-yl]-2-phenyl-ethane-1,2-dione

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