Technology Process of C22H29BrO3
There total 9 articles about C22H29BrO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
platinum(IV) oxide; hydrogen;
In
ethyl acetate;
at 23 ℃;
for 0.5h;
under 760.051 Torr;
DOI:10.1002/anie.201101842
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,2-dichloro-benzene / 3 h / 250 °C / Microwave irradiation; Inert atmosphere
2: platinum(IV) oxide; hydrogen / ethyl acetate / 0.5 h / 23 °C / 760.05 Torr
With
platinum(IV) oxide; hydrogen;
In
ethyl acetate; 1,2-dichloro-benzene;
DOI:10.1002/anie.201101842
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: acetonitrile; acetone / 22.5 h / Irradiation; quartz test tubes
1.2: 0.5 h
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 40 °C / Inert atmosphere
3.1: sodium t-butanolate / bis(tri-t-butylphosphine)palladium(0) / 7.5 h / 120 °C / Inert atmosphere; microwave
4.1: bromine / chloroform
5.1: 1,2-dichloro-benzene / 3 h / 250 °C / Inert atmosphere; microwave
6.1: hydrogen / platinum(IV) oxide / ethyl acetate / 0.5 h / 23 °C / 760.05 Torr
With
tetrabutyl ammonium fluoride; hydrogen; bromine; sodium t-butanolate;
platinum(IV) oxide; bis(tri-t-butylphosphine)palladium(0);
In
tetrahydrofuran; chloroform; ethyl acetate; 1,2-dichloro-benzene; acetone; acetonitrile;
