Technology Process of C28H37N5O4
There total 5 articles about C28H37N5O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C28H37N5O5;
With
acetic anhydride; acetic acid;
for 0.5h;
With
palladium 10% on activated carbon; hydrogen;
for 12h;
under 2585.81 - 2844.39 Torr;
DOI:10.1016/j.bioorg.2020.103856
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.17 h
1.2: 16 h / 20 °C
2.1: hydrogenchloride / methanol; water / 3 h / 0 - 20 °C
3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.17 h
3.2: 16 h / 20 °C
4.1: hydroxylamine hydrochloride / methanol / 0.17 h
4.2: 18 h
5.1: acetic acid; acetic anhydride / 0.5 h
5.2: 12 h / 2585.81 - 2844.39 Torr
With
hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; hydroxylamine hydrochloride; acetic anhydride; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bioorg.2020.103856
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydroxylamine hydrochloride / methanol / 0.17 h
1.2: 18 h
2.1: acetic acid; acetic anhydride / 0.5 h
2.2: 12 h / 2585.81 - 2844.39 Torr
With
hydroxylamine hydrochloride; acetic anhydride; acetic acid;
In
methanol;
DOI:10.1016/j.bioorg.2020.103856
