(R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Base Information

• Chemical Name: (R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate
• CAS No.: 1219799-61-7
• Molecular Formula: C₂₀H₃₂N₂O₄
• Molecular Weight: 364.485

Synonyms:(R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Chemical Property of (R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate

Chemical Property:

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Technology Process of (R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate

There total 1 articles about (R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C21H32N2O5 (1219799-56-0) → (R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate (1219799-61-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.01.035

Reference yield: 88.0%

(R)-tert-butyl 4-(((S)-1-hydroxy-3-phenylpropan-2-ylamino)methyl)-2,2-dimethyloxazolidine-3-carboxylate (1219799-61-7) + p-toluenesulfonyl chloride (98-59-9) → (R)-tert-butyl 2,2-dimethyl-4-((4-methyl-N-((S)-1-phenyl-3-(tosyloxy)propan-2-yl)phenylsulfonamido)methyl)oxazolidine-3-carboxylate (1219799-68-4)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1016/j.tetlet.2010.01.035

upstream raw materials:

C₂₁H₃₂N₂O₅

Downstream raw materials:

(R)-tert-butyl 2,2-dimethyl-4-((4-methyl-N-((S)-1-phenyl-3-(tosyloxy)propan-2-yl)phenylsulfonamido)methyl)oxazolidine-3-carboxylate

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