racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside

Base Information

• Chemical Name: racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside
• CAS No.: 131154-07-9
• Molecular Formula: C₁₆H₂₇NO₅
• Molecular Weight: 313.394

Synonyms:racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside

Chemical Property of racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside

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Technology Process of racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside

There total 3 articles about racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

methyl (2S,4R)-(+/-)-4-benzoylamino-2-ethoxy-3,4-dihydro-2H-pyran-6-carboxylate (110914-36-8) → racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside (131154-07-9) + (2R,4S,6R)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-07-9,131154-08-0) + (2R,4R,6S)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-07-9,131154-08-0) + (2R,4R,6R)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-08-0)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol; acetic acid; for 12h; under 37503 Torr; Yields of byproduct given;

Reference yield: 70.0%

methyl (2S,4R)-(+/-)-4-benzoylamino-2-ethoxy-3,4-dihydro-2H-pyran-6-carboxylate (110914-36-8) → racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside (131154-07-9) + (2R,4S,6R)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-07-9,131154-08-0) + (2R,4R,6S)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-07-9,131154-08-0) + (2R,4R,6R)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-08-0)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol; acetic acid; for 12h; under 37503 Torr; Yields of byproduct given;

Reference yield: 70.0%

methyl (2S,4R)-(+/-)-4-benzoylamino-2-ethoxy-3,4-dihydro-2H-pyran-6-carboxylate (110914-36-8) → racemic methyl N-cyclohexylcarbonyl-2-deoxy-3-epi-ezoaminuroate β-ethyl glycoside (131154-07-9) + (2R,4S,6R)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-07-9,131154-08-0) + (2R,4R,6S)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-07-9,131154-08-0) + (2R,4R,6R)-4-(Cyclohexanecarbonyl-amino)-6-ethoxy-tetrahydro-pyran-2-carboxylic acid methyl ester (131154-08-0)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol; acetic acid; for 12h; under 37503 Torr; Yields of byproduct given;

upstream raw materials:

methyl (2S,4R)-(+/-)-4-benzoylamino-2-ethoxy-3,4-dihydro-2H-pyran-6-carboxylate

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