5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate

Base Information

Chemical Name:5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate
CAS No.:205369-89-7
Molecular Formula:C₁₄H₂₀Cl₂N₃O₇P
Molecular Weight:444.208
Hs Code.:

Synonyms:5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate

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Technology Process of 5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate

There total 3 articles about 5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42454-06-8
2-nitro-5-hydroxybenzaldehyde

: 205369-89-7
5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / sodium hydroxide, sodium borohydride / ethanol / 4 h

2: 1.) NaOH / 1.) methanol, room temperature, 15 h, 2.) methanol, reflux, 15 h

With sodium hydroxide; sodium tetrahydroborate; In ethanol;
DOI:10.1021/jo961861m

Reference yield:

: 60463-12-9
3-hydroxymethyl-4-nitrophenol

: 205369-89-7
5-[(carbomethoxy)methoxy]-2-nitrobenzyl N,N-bis(2-chloroethyl)phosphordiamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOH / 1.) methanol, room temperature, 15 h, 2.) methanol, reflux, 15 h

With sodium hydroxide;
DOI:10.1021/jo961861m