Technology Process of C42H64O7
There total 20 articles about C42H64O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 10h;
DOI:10.1039/c3ob42364f
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: mercury(II) oxide; mercury dichloride / water; acetone / 60 °C
2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 - 20 °C
3.1: acetic acid / water / 20 °C
4.1: triethylamine; di(n-butyl)tin oxide / dichloromethane / 20 °C
5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 10 h / Reflux
6.1: n-butyllithium / tetrahydrofuran / 3 h / -78 - -20 °C
6.2: -78 °C
7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; potassium tert-butylate; tetrabutyl ammonium fluoride; di(n-butyl)tin oxide; acetic acid; triethylamine; mercury dichloride; mercury(II) oxide;
In
tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1039/c3ob42364f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine; di(n-butyl)tin oxide / dichloromethane / 20 °C
2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 10 h / Reflux
3.1: n-butyllithium / tetrahydrofuran / 3 h / -78 - -20 °C
3.2: -78 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C
With
tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; tetrabutyl ammonium fluoride; di(n-butyl)tin oxide; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c3ob42364f