(R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate

Base Information

Chemical Name:(R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate
CAS No.:1280225-69-5
Molecular Formula:C₄₁H₃₈N₂O₅S
Molecular Weight:670.829
Hs Code.:

Synonyms:(R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate

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Chemical Property of (R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate

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Technology Process of (R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate

There total 4 articles about (R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1280225-73-1
C₄₇H₄₄N₂O₆S

: 459-73-4
GlyOEt*HCl

: 1280225-69-5
(R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; for 10.0833h;
DOI:10.1016/j.tetasy.2010.12.021

Reference yield: 77.0%

: 623-33-6
glycine ethyl ester hydrochloride

: 103213-32-7,167015-11-4
N-(9-fluorenylmethoxycarbonyl)-S-trityl-L-cysteine

: 1280225-69-5
(R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate

Guidance literature:: With dmap; Bromotrichloromethane; In 1,2-dichloro-ethane; at 20 ℃; for 1h; Irradiation;
DOI:10.1002/anie.202011510

Reference yield: 73.0%

: 637-81-0
ethyl-2-azidoacetate

: 103213-32-7,167015-11-4
N-(9-fluorenylmethoxycarbonyl)-S-trityl-L-cysteine

: 1280225-69-5
(R)-ethyl 2-(2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(tritylthio)propanamido)acetate

Guidance literature:: With sodium hydride; chloro-diphenylphosphine; In chlorobenzene; at 20 - 80 ℃; for 14h; chemoselective reaction;
DOI:10.1002/chem.201201773