(Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone

Base Information

• Chemical Name: (Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone
• CAS No.: 147438-12-8
• Molecular Formula: C₁₅H₁₉NO₂Si
• Molecular Weight: 273.407
• Mol file: 147438-12-8.mol

Synonyms:(Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone

Chemical Property of (Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone

Chemical Property:

Purity/Quality:

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Technology Process of (Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone

There total 1 articles about (Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

carbon monoxide (201230-82-2) + Dimethylphenylsilane (766-77-8) + 5-ethynyl-2-pyrrolidinone (105457-63-4) → (Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone (147438-12-8)

Guidance literature:

acetylacetonatodicarbonylrhodium(l); In toluene; for 24h; under 15514.4 Torr; Product distribution; Ambient temperature; other catalysts;

DOI:10.1016/S0040-4039(00)77453-3

Reference yield: 100.0%

(Z)-5-<(2-dimethylphenylsilyl-1-formyl)ethenyl>pyrrolidinone (147438-12-8) → 5-(1-Hydroxymethyl-2-dimethylphenylsilylethenyl)-2-pyrrolidinone

Guidance literature:

With sodium tetrahydroborate; In ethanol; water; 0 deg C - room temperature, overnight;

DOI:10.1016/S0040-4039(00)77453-3

upstream raw materials:

carbon monoxide

Dimethylphenylsilane

5-ethynyl-2-pyrrolidinone