Technology Process of C31H32O8S
There total 8 articles about C31H32O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl-ammonium chloride; sodium tris(acetoxy)borohydride;
In
1,2-dimethoxyethane; toluene;
at 80 ℃;
DOI:10.1055/s-0032-1317920
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 0 - 20 °C
2: trimethylsilyl iodide / toluene; acetonitrile / 60 °C
3: sodium tris(acetoxy)borohydride; tetrabutyl-ammonium chloride / toluene; 1,2-dimethoxyethane / 80 °C
With
trimethylsilyl iodide; tetrabutyl-ammonium chloride; sodium tris(acetoxy)borohydride; lithium hexamethyldisilazane;
In
tetrahydrofuran; 1,2-dimethoxyethane; toluene; acetonitrile;
DOI:10.1055/s-0032-1317920
-
-
3-[(3aR,5R,6S,6aR)-6-benzyloxy-2,2-dimethyl-3a,5,6,6a-tetrahydrofuro[2,3-d][1,3]dioxol-5-yl]propane-1,2-diol
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap; 4-methyl-morpholine / toluene / 75 °C
2: titanium tetrachloride; titanium(IV) isopropylate / toluene / 25 °C
3: trichloroacetic acid anhydride; triethylamine / toluene; dimethyl sulfoxide / -10 °C
4: lithium hexamethyldisilazane / toluene; tetrahydrofuran / 0 - 20 °C
5: trimethylsilyl iodide / toluene; acetonitrile / 60 °C
6: sodium tris(acetoxy)borohydride; tetrabutyl-ammonium chloride / toluene; 1,2-dimethoxyethane / 80 °C
With
4-methyl-morpholine; titanium(IV) isopropylate; dmap; trimethylsilyl iodide; tetrabutyl-ammonium chloride; titanium tetrachloride; sodium tris(acetoxy)borohydride; triethylamine; lithium hexamethyldisilazane; trichloroacetic acid anhydride;
In
tetrahydrofuran; 1,2-dimethoxyethane; dimethyl sulfoxide; toluene; acetonitrile;
3: |Swern Oxidation;
DOI:10.1055/s-0032-1317920