methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate

Base Information

Chemical Name:methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate
CAS No.:433226-40-5
Molecular Formula:C₁₉H₂₁N₅O₅
Molecular Weight:399.406
Hs Code.:

Synonyms:methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate

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Chemical Property of methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate

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Technology Process of methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate

There total 4 articles about methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 433226-05-2
5-bromo-2-nitropyridine-3-ylamine

: 433226-40-5
methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 624 mg / Cs₂CO₃ / dimethylformamide / 72 h / 20 °C

2: aq. Na₂S₂O₄ / ethanol / Heating

3: ethanol / Heating

With sodium dithionite; caesium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0611051

Reference yield:

: 152684-24-7
3-bromo-5-(ethoxycarbonyl)aminopyridine

: 433226-40-5
methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: 54 percent / H₂SO₄; aq. HNO₃ / 0 - 20 °C

2: aq. KOH / ethanol / 1 h / 90 °C

3: 624 mg / Cs₂CO₃ / dimethylformamide / 72 h / 20 °C

4: aq. Na₂S₂O₄ / ethanol / Heating

5: ethanol / Heating

With potassium hydroxide; sodium dithionite; sulfuric acid; nitric acid; caesium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0611051

Reference yield:

: 152684-25-8
3-bromo-5-(ethoxycarbonyl)amino-2-nitropyridine

: 433226-40-5
methyl (5-(4-(tert-butoxycarbonyl)aminophenoxy)-3,7-diazaindole-2-yl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: aq. KOH / ethanol / 1 h / 90 °C

2: 624 mg / Cs₂CO₃ / dimethylformamide / 72 h / 20 °C

3: aq. Na₂S₂O₄ / ethanol / Heating

4: ethanol / Heating

With potassium hydroxide; sodium dithionite; caesium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0611051