2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine

Base Information

Chemical Name:2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine
CAS No.:1609182-87-7
Molecular Formula:C₁₇H₁₇NO₄S₂
Molecular Weight:363.458
Hs Code.:

Synonyms:2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine

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Chemical Property of 2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine

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Technology Process of 2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine

There total 2 articles about 2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1609182-71-9
2-hydroxyimino-3-oxo-3-p-tolyl-dithiopropionic acid methyl ester

: 762-21-0
acetylenedicarboxylic acid diethyl ester

: 1609182-87-7
2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine

Guidance literature:: DOI:10.1016/j.tet.2014.03.097

Reference yield:

: 37510-36-4
methyl 3-hydroxy-3-(p-methylphenyl)prop-2-enedithioate

: 1609182-87-7
2-carboethoxy methylene-5-(4-methyl-benzoyl)-6-methylsulfanyl-3-oxo-1,4-thiazine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium nitrite / methanol / 0.5 h / Cooling with ice

With hydrogenchloride; sodium nitrite; In methanol;
DOI:10.1016/j.tet.2014.03.097