menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

Base Information

Chemical Name:menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate
CAS No.:158419-31-9
Molecular Formula:C₂₂H₄₀N₂O₄Si
Molecular Weight:424.656
Hs Code.:

Synonyms:menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

Suppliers and Price of menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

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Chemical Property of menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

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Technology Process of menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

There total 5 articles about menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 63254-60-4,80655-94-3,120143-37-5
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-aminoacetate

: 82938-50-9,162856-35-1
(4S)-N-tert-butyldimethylsilylazetidin-2-one-4-carboxylic acid

: 158419-31-9
menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)85061-4

Reference yield:

: 2216-51-5
(-)-menthol

: 158419-31-9
menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / DMAP, DCC / CH₂Cl₂ / Ambient temperature

2: 88 percent / H₂ / 5percent Pd-C / methanol / 3 h / Ambient temperature

3: 88 percent / DMAP, DCC / CH₂Cl₂ / Ambient temperature

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)85061-4

Reference yield:

: 82938-49-6
benzyl (S)-1-(tert-butyldimethylsilyl)-4-oxoazetidine-2-carboxylate

: 158419-31-9
menthyl N-<1-tert-butyldimethylsilyl-2-azetidinone-4-carboxy>glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / H₂ / 5percent Pd-C / methanol / 1 h / 3102.9 Torr / Ambient temperature

2: 88 percent / DMAP, DCC / CH₂Cl₂ / Ambient temperature

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(01)85061-4