titanocene pentaselenide

Base Information Edit

Chemical Name:titanocene pentaselenide
CAS No.:12307-22-1
Molecular Formula:C₁₀H₁₀Se₅Ti
Molecular Weight:572.869
Hs Code.:
Mol file:12307-22-1.mol

Synonyms:titanocene pentaselenide

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Chemical Property of titanocene pentaselenide Edit

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Technology Process of titanocene pentaselenide

There total 1 articles about titanocene pentaselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.2%

: bis(cyclopentadienyl)-titanium(III) chloride

: selenium

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 12307-22-1
titanocene pentaselenide

Guidance literature:: In tetrahydrofuran; Se powder was added to a stirred soln. of the complex under Ar; the mixt. became red brown in a few minutes; it was stirred for 4 h, the excessof Se was filtered off, the filtrate was concd. and chromd. on SiO2; isolated by flash chromy. on SiO2;

Reference yield: 90.0%

: 12307-22-1
titanocene pentaselenide

: 762-42-5
dimethyl acetylenedicarboxylate

: 7782-49-2
selenium

: 82865-10-9
[(C₅H₅)2TiSe₂C₂(CO₂CH₃)2]

Guidance literature:: In xylene; under N2, xylene soln. of Ti complex and dimethyl acetylenedicarboxylate refluxed for 0.5 h; cooled, filtered, Se washed with CH2Cl2, filtrate evapd. to oil, dissolved in small amt. of CH2Cl2, chromd., diluted with CH2Cl2, concd. in vac., cooled at -20°C, filtered;