(R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol

Base Information

Chemical Name:(R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol
CAS No.:1201522-87-3
Molecular Formula:C₂₀H₂₄O₄S
Molecular Weight:360.474
Hs Code.:

Synonyms:(R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol

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Chemical Property of (R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol

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Technology Process of (R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol

There total 1 articles about (R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1201522-79-3
(2R,3R,4S)-6-(benzyloxy)-4-bromo-1-(S(S))-(p-tolylsulfinyl)hexane-2,3-diol

: 1201522-87-3
(R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol

Guidance literature:: With potassium carbonate; In acetonitrile; at 0 - 20 ℃; for 8.25h; Inert atmosphere;
DOI:10.1016/j.tet.2009.09.062

Reference yield: 81.0%

: 1201522-87-3
(R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1201522-75-9
C₂₆H₃₈O₄SSi

Guidance literature:: With 1H-imidazole; In dichloromethane;
DOI:10.1016/j.tet.2009.09.062

Reference yield: 41.0%

: 1201522-87-3
(R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol

: 1201522-89-5
(2R,4R)-6-(benzyloxy)-1-(S(S))-(p-tolylsulfinyl)hexane-2,4-diol

Guidance literature:: (R)-1-{(2R,3R)-3-[2-(benzyloxy)ethyl]oxiran-2-yl}-2-(S(S))-(p-tolylsulfinyl)ethanol; With bis(cyclopentadienyl)titanium dichloride; zinc(II) chloride; zinc; In tetrahydrofuran; at -23 - 0 ℃; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; at 0 ℃;
DOI:10.1016/j.tet.2009.09.062