N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine

Base Information

Chemical Name:N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine
CAS No.:588719-12-4
Molecular Formula:C₂₉H₃₃N₅O₅
Molecular Weight:531.612
Hs Code.:

Synonyms:N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine

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Chemical Property of N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine

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Technology Process of N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine

There total 3 articles about N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 588719-10-2
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine methyl ester

: 588719-12-4
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 4h;
DOI:10.1039/b212470j

Reference yield:

: 20691-84-3
m-methyl red

: 588719-12-4
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / DCC; HOBt / dimethylformamide

2: 98 percent / aq. NaOH / dioxane / 4 h / 20 °C

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/b212470j

Reference yield:

: 26348-68-5
N-(benzyloxycarbonyl)lysine methyl ester hydrochloride

: 588719-12-4
N-benzyloxycarbonyl-ω-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}lysine

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / DCC; HOBt / dimethylformamide

2: 98 percent / aq. NaOH / dioxane / 4 h / 20 °C

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1039/b212470j