Technology Process of C14H20O
There total 5 articles about C14H20O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
dichloromethane;
at 20 ℃;
for 24h;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: water; lithium hydroxide / tetrahydrofuran / 20 °C
2.1: dmap / dichloromethane / 2 h / 20 °C
3.1: aluminum (III) chloride / carbon disulfide / 20 - 70 °C
4.1: magnesium / iodine / diethyl ether / 20 °C / Inert atmosphere
4.2: 0 °C / Inert atmosphere; Reflux
4.3: 0 °C
5.1: toluene-4-sulfonic acid / dichloromethane / 24 h / 20 °C
With
dmap; aluminum (III) chloride; water; toluene-4-sulfonic acid; magnesium; lithium hydroxide;
iodine;
In
tetrahydrofuran; carbon disulfide; diethyl ether; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: dmap / dichloromethane / 2 h / 20 °C
2.1: aluminum (III) chloride / carbon disulfide / 20 - 70 °C
3.1: magnesium / iodine / diethyl ether / 20 °C / Inert atmosphere
3.2: 0 °C / Inert atmosphere; Reflux
3.3: 0 °C
4.1: toluene-4-sulfonic acid / dichloromethane / 24 h / 20 °C
With
dmap; aluminum (III) chloride; toluene-4-sulfonic acid; magnesium;
iodine;
In
carbon disulfide; diethyl ether; dichloromethane;