4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol

Base Information

Chemical Name:4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol
CAS No.:78826-17-2
Molecular Formula:C₁₇H₂₀N₂O₈S
Molecular Weight:412.42
Hs Code.:

Synonyms:4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol

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Chemical Property of 4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol

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Technology Process of 4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol

There total 3 articles about 4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 69920-06-5
2-(2-Methoxyethoxy)-5-nitrobenzenesulfonyl chloride

: 84011-45-0
2-amino-4-methoxy-5-methylphenol hydrochloride

: 78826-17-2
4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol

Guidance literature:: With pyridine; In N,N-dimethyl acetamide; for 2h; Ambient temperature;
DOI:10.1021/jo00150a008

Reference yield:

: 66481-29-6
2,6-dimethyl-5-hydroxybenzoxazole

: 78826-17-2
4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium methoxide

2: 80 percent / 35percent HCl / ethanol / 1 h / Heating

3: 57 percent / pyridine / N,N-dimethyl-acetamide / 2 h / Ambient temperature

With pyridine; hydrogenchloride; sodium methylate; In ethanol; N,N-dimethyl acetamide;
DOI:10.1021/jo00150a008

Reference yield:

: 84011-43-8
2,6-dimethyl-5-methoxybenzoxazole

: 78826-17-2
4-methoxy-2-<<2-(2-methoxyethoxy)-5-nitrophenyl>-sulfonamido>-5-methylphenol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 35percent HCl / ethanol / 1 h / Heating

2: 57 percent / pyridine / N,N-dimethyl-acetamide / 2 h / Ambient temperature

With pyridine; hydrogenchloride; In ethanol; N,N-dimethyl acetamide;
DOI:10.1021/jo00150a008