(Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

Base Information

Chemical Name:(Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene
CAS No.:137540-60-4
Molecular Formula:C₁₇H₁₈OS₂
Molecular Weight:302.461
Hs Code.:

Synonyms:(Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

Suppliers and Price of (Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

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Technology Process of (Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

There total 4 articles about (Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 13596-95-7
2-methyl-4-(phenylthio)but-3-yn-2-ol

: 108-98-5
thiophenol

: 137540-60-4
(Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

Guidance literature:: With cesium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 5h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/cjoc.201190154

Reference yield: 89.0%

: 115-19-5
2-methyl-but-3-yn-2-ol

: 882-33-7
diphenyldisulfane

: 137540-60-4
(Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 80 ℃; for 12h;
DOI:10.1021/ja00026a013

Reference yield: 72.0%

: 59-88-1
phenylhydrazine hydrochloride

: 115-19-5
2-methyl-but-3-yn-2-ol

: 137540-60-4
(Z)-1,2-bis(phenylthio)-3-hydroxy-3-methyl-1-butene

Guidance literature:: With NHC-Pd(II)-Im; dihydrogen peroxide; caesium carbonate; sodium thiosulfate; at 120 ℃; for 12h; regioselective reaction; Ionic liquid; Inert atmosphere;
DOI:10.1039/d1ra05773a