1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone

Base Information

Chemical Name:1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone
CAS No.:80716-70-7
Molecular Formula:C₃₄H₃₀O₄
Molecular Weight:502.61
Hs Code.:

Synonyms:1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone

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Chemical Property of 1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone

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Technology Process of 1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone

There total 5 articles about 1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 80716-64-9
4-carboxy-1,3-bis(α-chloro-α-hydroxybenzyl)-2,5-diphenylcyclopentaneacetic acid di-γ-lactone

: 80716-70-7
1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone

Guidance literature:: With hydrogen; palladium on activated charcoal; for 60h; under 2068.6 Torr; Ambient temperature;
DOI:10.1021/jo00134a014

Reference yield:

: 80716-69-4
dimethyl 1,3-dibenzoyl-2,5-diphenylcyclopentane-cis-1,4-diacetate

: 80716-70-7
1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 3102.9 Torr;
DOI:10.1016/S0040-4039(01)82018-9

Reference yield:

: 80716-63-8
3-Benzoyl 4-Phenylisocrotonic acid

: 80716-70-7
1-(α-hydroxybenzyl)-3-benzyl-cis-4-carboxy-2,5-diphenylcyclopentaneacetic acid γ-lactone

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / 1.) RT, 7 d, 2.) C₆H₆, CH₂C₂, reflux, 20 h

2: 57 percent / H₂ / 10percent Pd/C / 60 h / 2068.6 Torr / Ambient temperature

With hydrogen; acetyl chloride; palladium on activated charcoal;
DOI:10.1021/jo00134a014