methyl 3,4,6-tri-O-benzyl-2-O-α-D-mannopyranosyl-α-D-mannopyranoside

Base Information Edit

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-O-α-D-mannopyranosyl-α-D-mannopyranoside
CAS No.:107937-20-2
Molecular Formula:C₃₄H₄₂O₁₁
Molecular Weight:626.701
Hs Code.:
Mol file:107937-20-2.mol

Synonyms:methyl 3,4,6-tri-O-benzyl-2-O-α-D-mannopyranosyl-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-O-α-D-mannopyranosyl-α-D-mannopyranoside Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-O-α-D-mannopyranosyl-α-D-mannopyranoside

There total 10 articles about methyl 3,4,6-tri-O-benzyl-2-O-α-D-mannopyranosyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3068-32-4
1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

: 107937-20-2,108399-90-2,131283-78-8
(2S,3R,4S,5R,6R)-2-((2R,3R,4S,5S,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-methoxy-tetrahydro-pyran-3-yloxy)-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 6 steps

1: 2,6-dimethylpyridine

2: sodium methoxide / methanol

3: silver oxide / dimethylformamide / 18 h

4: 1.) p-toluenesulfonic acid, 2.) sodium methoxide / 1.) methanol, 30 min, 50 deg C

5: silver carbonate / CH₂Cl₂ / 2 h

6: sodium methoxide / methanol

With 2,6-dimethylpyridine; sodium methylate; toluene-4-sulfonic acid; silver carbonate; silver(l) oxide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)80790-9