methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside

Base Information

Chemical Name:methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside
CAS No.:131283-80-2
Molecular Formula:C₄₆H₅₁O₁₄P
Molecular Weight:858.876
Hs Code.:

Synonyms:methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside

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Chemical Property of methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside

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Technology Process of methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside

There total 4 articles about methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 131283-78-8
methyl 3,4,5-tri-O-benzyl-2-O-(α-D-mannopyranosyl)-β-D-mannopyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 131283-80-2
methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside

Guidance literature:: In pyridine; at 0 ℃; for 2h;
DOI:10.1016/0008-6215(90)80005-N

Reference yield: 55.5%

: 107937-20-2
methyl 3,4,6-tri-O-benzyl-2-O-α-D-mannopyranosyl-α-D-mannopyranoside

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 131283-80-2
Phosphoric acid (2R,3S,4S,5S,6R)-6-((2S,3S,4S,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-2-methoxy-tetrahydro-pyran-3-yloxy)-3,4,5-trihydroxy-tetrahydro-pyran-2-ylmethyl ester diphenyl ester

Guidance literature:: With pyridine; at 0 ℃;
DOI:10.1016/0008-6215(86)80026-X

Reference yield:

: 73415-91-5
methyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

: 131283-80-2
methyl 3,4,6-tri-O-benzyl-2-O-<α-D-mannopyranosyl 6-(diphenyl phosphate)>-β-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Hg(CN)2 2) 0.05 M NaOMe / 1) benzene, nitromethane, 50 to 55 deg C 2) MeOH, r.t., 3 h

2: 75 percent / pyridine / 2 h / 0 °C

With sodium methylate; mercury(II) cyanide; In pyridine;
DOI:10.1016/0008-6215(90)80005-N