2-(2-Chlorophenyl)ethyl 4-methylbenzene-1-sulfonate

Base Information

Chemical Name:2-(2-Chlorophenyl)ethyl 4-methylbenzene-1-sulfonate
CAS No.:119779-14-5
Molecular Formula:C₁₅H₁₅ClO₃S
Molecular Weight:310.801
Hs Code.:
DSSTox Substance ID:DTXSID101206949

Synonyms:119779-14-5;2-(2-chlorophenyl)ethyl 4-methylbenzene-1-sulfonate;SCHEMBL8209789;DTXSID101206949;EN300-7202502;Benzeneethanol, 2-chloro-, 1-(4-methylbenzenesulfonate)

Suppliers and Price of 2-(2-Chlorophenyl)ethyl 4-methylbenzene-1-sulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Chlorophenyl)ethyl 4-methylbenzene-1-sulfonate

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:310.0430432
Heavy Atom Count:20
Complexity:382

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)OCCC2=CC=CC=C2Cl

Technology Process of 2-(2-Chlorophenyl)ethyl 4-methylbenzene-1-sulfonate

There total 3 articles about 2-(2-Chlorophenyl)ethyl 4-methylbenzene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19819-95-5
2-(2-chlorophenyl)-1-ethanol

: 98-59-9
p-toluenesulfonyl chloride

: 119779-14-5
2-chlorophenethyl 4-methylbenzenesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1039/b618875c

Reference yield:

: 2444-36-2
2'-chloro-benzeneacetic acid

: 119779-14-5
2-chlorophenethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 4.5 h / 0 - 20 °C / Inert atmosphere

3: pyridine / 4 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2017.05.012

Reference yield:

: 57486-68-7
methyl (2-chlorophenyl)acetate

: 119779-14-5
2-chlorophenethyl 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 4.5 h / 0 - 20 °C / Inert atmosphere

2: pyridine / 4 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2017.05.012